E-ISSN 0976-2779 | ISSN 0975-8453
 

Review Article 


Synthesis and Antibacterial Evaluation of Some Azo-Schiff Base Ligands and Estimation the Cadmium Metal by Complexation

Ekhlas Q. Jasim, Erfan A. Alasadi, Rajaa H. Fayadh, Munther A. Muhamman-Ali.

Abstract
The present paper describes the synthesis of four azo-Schiff base named (1a-4a) by diazotization reaction of the synthesized Schiff bases with sulfonamide compound. All new synthesized derivatives were identified by melting points, CHNS, FT-IR and 1H-NMR spectra. All compounds were tested for their antibacterial activity that showed good activity. The synthesized compounds were used as sensitive and selective analytical reagent for the spectrophotometric determination of cadmium (II). The calibration curve is linear between 0.05 and 30 μg.ml-1 and limit of quantification, LOQ of (1.203, 1.078, 1.443 and 0.875) μg.ml-1 with molar absorptivity and Sandal's sensitivity values of ligands 2.4778x104, 1.6740x104, 1.70019x104, 1.9002 x104 L mol-1 cm-1 (0.049x10-4, 0.169x10-4, 0.132x10-4, 0.110 x10-4 µg.cm-2, for 1a, 2a, 3a and 4a, respectively. The composition of the Cd (II) - (1a, 2a, 3a and 4a) complex is established as 1:2 by molar ratio and job methods. An excellent linearity with a correlation coefficient value of (0.9997, 0.9996, 0.9974 and 0.9985) is obtained for the complexes.

Key words: Azo-Schiff base, Cadmium, diazotization, Absorption spectra, Mole ratio


 
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How to Cite this Article
Pubmed Style

Ekhlas Q. Jasim, Erfan A. Alasadi, Rajaa H. Fayadh, Munther A. Muhamman-Ali. Synthesis and Antibacterial Evaluation of Some Azo-Schiff Base Ligands and Estimation the Cadmium Metal by Complexation. SRP. 2020; 11(6): 677-687. doi:10.31838/srp.2020.6.101


Web Style

Ekhlas Q. Jasim, Erfan A. Alasadi, Rajaa H. Fayadh, Munther A. Muhamman-Ali. Synthesis and Antibacterial Evaluation of Some Azo-Schiff Base Ligands and Estimation the Cadmium Metal by Complexation. http://www.sysrevpharm.org//?mno=118812 [Access: June 25, 2020]. doi:10.31838/srp.2020.6.101


AMA (American Medical Association) Style

Ekhlas Q. Jasim, Erfan A. Alasadi, Rajaa H. Fayadh, Munther A. Muhamman-Ali. Synthesis and Antibacterial Evaluation of Some Azo-Schiff Base Ligands and Estimation the Cadmium Metal by Complexation. SRP. 2020; 11(6): 677-687. doi:10.31838/srp.2020.6.101



Vancouver/ICMJE Style

Ekhlas Q. Jasim, Erfan A. Alasadi, Rajaa H. Fayadh, Munther A. Muhamman-Ali. Synthesis and Antibacterial Evaluation of Some Azo-Schiff Base Ligands and Estimation the Cadmium Metal by Complexation. SRP. (2020), [cited June 25, 2020]; 11(6): 677-687. doi:10.31838/srp.2020.6.101



Harvard Style

Ekhlas Q. Jasim, Erfan A. Alasadi, Rajaa H. Fayadh, Munther A. Muhamman-Ali (2020) Synthesis and Antibacterial Evaluation of Some Azo-Schiff Base Ligands and Estimation the Cadmium Metal by Complexation. SRP, 11 (6), 677-687. doi:10.31838/srp.2020.6.101



Turabian Style

Ekhlas Q. Jasim, Erfan A. Alasadi, Rajaa H. Fayadh, Munther A. Muhamman-Ali. 2020. Synthesis and Antibacterial Evaluation of Some Azo-Schiff Base Ligands and Estimation the Cadmium Metal by Complexation. Systematic Reviews in Pharmacy, 11 (6), 677-687. doi:10.31838/srp.2020.6.101



Chicago Style

Ekhlas Q. Jasim, Erfan A. Alasadi, Rajaa H. Fayadh, Munther A. Muhamman-Ali. "Synthesis and Antibacterial Evaluation of Some Azo-Schiff Base Ligands and Estimation the Cadmium Metal by Complexation." Systematic Reviews in Pharmacy 11 (2020), 677-687. doi:10.31838/srp.2020.6.101



MLA (The Modern Language Association) Style

Ekhlas Q. Jasim, Erfan A. Alasadi, Rajaa H. Fayadh, Munther A. Muhamman-Ali. "Synthesis and Antibacterial Evaluation of Some Azo-Schiff Base Ligands and Estimation the Cadmium Metal by Complexation." Systematic Reviews in Pharmacy 11.6 (2020), 677-687. Print. doi:10.31838/srp.2020.6.101



APA (American Psychological Association) Style

Ekhlas Q. Jasim, Erfan A. Alasadi, Rajaa H. Fayadh, Munther A. Muhamman-Ali (2020) Synthesis and Antibacterial Evaluation of Some Azo-Schiff Base Ligands and Estimation the Cadmium Metal by Complexation. Systematic Reviews in Pharmacy, 11 (6), 677-687. doi:10.31838/srp.2020.6.101





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