Synthesis, Characterization and Corrosion Inhibition Study of New Heterocyclic Compounds and Schiff Base with [Co (II), Ni (II), Cu (II) and Hg (II)] Complexes
Abstract
Wurood Ali Jaafar and Ruwaidah S. Saeed
In the present research, 4-aminoacetophenon reaction with benzoin in ethanol to procure compound [1]. Compound [1] was reacted with 4-aminobenzenesulfonamide and few drops from (glacial CH3COOH) in EtOH to yield compound [2]. Compound [2] reaction with 2-mercaptobenzoic acid or sodium azide or various anhydrides to give Thiazine [3], tetrazole [4] and 1,3- oxazepine derivatives [5,6] respectively.
The structure of synthesized compounds identified by spectral data (FT-IR), (1H-NMR) spectra and analysis (CHN-S). The Schiff base ligand and synthesis some transition metals complexes [Co (II), Ni (II), Cu (II) and Hg (II) of this ligand were described via FTIR, UV-Visible Spectroscopy and the elemental analysis (CHN-S). in our coclusion we found The corrosion inhibition study of Thiazine [3] tetrazole [4] 1,3- oxazepine[5] ligand and their complexes on mild steel in (0.1M) hydrochloric acid were researched by weight loss .
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| Pubmed Style Wurood Ali Jaafar and Ruwaidah S. Saeed. Synthesis, Characterization and Corrosion Inhibition Study of New Heterocyclic Compounds and Schiff Base with [Co (II), Ni (II), Cu (II) and Hg (II)] Complexes. SRP. 2020; 11(10): 134-143. doi:10.31838/srp.2020.10.23 Web Style Wurood Ali Jaafar and Ruwaidah S. Saeed. Synthesis, Characterization and Corrosion Inhibition Study of New Heterocyclic Compounds and Schiff Base with [Co (II), Ni (II), Cu (II) and Hg (II)] Complexes. http://www.sysrevpharm.org/?mno=10543 [Access: March 28, 2021]. doi:10.31838/srp.2020.10.23 AMA (American Medical Association) Style Wurood Ali Jaafar and Ruwaidah S. Saeed. Synthesis, Characterization and Corrosion Inhibition Study of New Heterocyclic Compounds and Schiff Base with [Co (II), Ni (II), Cu (II) and Hg (II)] Complexes. SRP. 2020; 11(10): 134-143. doi:10.31838/srp.2020.10.23 Vancouver/ICMJE Style Wurood Ali Jaafar and Ruwaidah S. Saeed. Synthesis, Characterization and Corrosion Inhibition Study of New Heterocyclic Compounds and Schiff Base with [Co (II), Ni (II), Cu (II) and Hg (II)] Complexes. SRP. (2020), [cited March 28, 2021]; 11(10): 134-143. doi:10.31838/srp.2020.10.23 Harvard Style Wurood Ali Jaafar and Ruwaidah S. Saeed (2020) Synthesis, Characterization and Corrosion Inhibition Study of New Heterocyclic Compounds and Schiff Base with [Co (II), Ni (II), Cu (II) and Hg (II)] Complexes. SRP, 11 (10), 134-143. doi:10.31838/srp.2020.10.23 Turabian Style Wurood Ali Jaafar and Ruwaidah S. Saeed. 2020. Synthesis, Characterization and Corrosion Inhibition Study of New Heterocyclic Compounds and Schiff Base with [Co (II), Ni (II), Cu (II) and Hg (II)] Complexes. Systematic Reviews in Pharmacy, 11 (10), 134-143. doi:10.31838/srp.2020.10.23 Chicago Style Wurood Ali Jaafar and Ruwaidah S. Saeed. "Synthesis, Characterization and Corrosion Inhibition Study of New Heterocyclic Compounds and Schiff Base with [Co (II), Ni (II), Cu (II) and Hg (II)] Complexes." Systematic Reviews in Pharmacy 11 (2020), 134-143. doi:10.31838/srp.2020.10.23 MLA (The Modern Language Association) Style Wurood Ali Jaafar and Ruwaidah S. Saeed. "Synthesis, Characterization and Corrosion Inhibition Study of New Heterocyclic Compounds and Schiff Base with [Co (II), Ni (II), Cu (II) and Hg (II)] Complexes." Systematic Reviews in Pharmacy 11.10 (2020), 134-143. Print. doi:10.31838/srp.2020.10.23 APA (American Psychological Association) Style Wurood Ali Jaafar and Ruwaidah S. Saeed (2020) Synthesis, Characterization and Corrosion Inhibition Study of New Heterocyclic Compounds and Schiff Base with [Co (II), Ni (II), Cu (II) and Hg (II)] Complexes. Systematic Reviews in Pharmacy, 11 (10), 134-143. doi:10.31838/srp.2020.10.23 |
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